Back to Explorer

CVM GFI #136 Protocols for the Conduct of Method Transfer Studies for Type C Medicated Feed Assay Methods

FinalCenter for Veterinary Medicine04/26/2007

Description

Section 512(b) of the Federal Food, Drug, and Cosmetic Act (the act) (21 U.S.C. §360b) establishes the requirements for a new animal drug approval. FDA regulations specify the information you (the sponsor) must submit as part of your new animal drug application (NADA) and the proper format for the NADA submission. 21 CFR 514.1. As part of your NADA submission, you must describe analytical procedures capable of determining the active component(s) of the new animal drug within a reasonable degree of accuracy and of assuring the identity of such components. 21 CFR 514.1(b)(5)(vii). This includes a description of practicable methods of analysis (assay methods) that have adequate sensitivity to determine the amount of the new animal drug in the final dosage form. 21 CFR 514.1(b)(5)(vii)(a). In the case of a Type A medicated article, the Type C medicated feed is a final dosage form used to treat the animal. Thus, as part of the NADA review process, FDA looks at assay methods for determining the amount of a new animal drug in Type C medicated feed.

Scope & Applicability

Product Classes

3
Type C Medicated Feed

Final feed administered to animals

Medicated Animal Feeds

The transfer study evaluates methods for drugs used in medicated animal feeds.

Type A Medicated Article

New animal drug dosage forms intended for use in the manufacture of medicated feeds; The primary product category discussed for CMC considerations.; manufactured for homogeneity, segregation, and stability studies

Stakeholders

10
Investigator

Responsible for qualifications, training, and trial conduct; Individual responsible for trial conduct and data governance at a site.; May delegate tasks but retains overall responsibility; Person responsible for the conduct of the clinical trial at a trial site; Responsible for trial conduct and participant safety; Responsible for trial conduct, data integrity, and investigational product management.; Individual responsible for trial conduct at a site and informing the institution.; maintaining

Sponsor Study Director

Individual communicating with the participating laboratory personnel.

Sponsor

Entity responsible for submitting applications under section 524B

Reference Laboratory

Expert laboratory with experience performing the assay method.; The reference laboratory may also provide a separate report.; The sponsor's expert laboratory or contract lab with experience in the assay method.

Participating Laboratory

Laboratory conducting the analytical phase of the transfer study.; Each participating laboratory should provide a report documenting their data.; The laboratory conducting the analytical phase of the transfer study.

State Feed Laboratory

Recommend that at least one of the laboratories be a state feed laboratory.

Sponsor's Study Director

The individual responsible for overseeing the conduct and evaluation of the study.

Qualified Person

individual responsible for evaluating potential risks

Participating Laboratory Study Coordinator

Personnel responsible for conducting the transfer study and evaluating results.

ONADE Representative

Person designated by ONADE to review the protocol and summary report.

Regulatory Context

Attributes

5
Expiration Date

Property of a device that may be changed via established protocols

Expiration Dates

Stability studies to justify assigned expiration or retest dates.

Storage Conditions

Long-term, accelerated, and intermediate conditions

Storage Stability

Consistent with the known storage stability of the drug in the feed.

Reference Concentration

The concentration of the drug substance as determined by the reference laboratory.

Related CFR Sections (2)

See Also (8)

CVM GFI #136 Protocols for the Conduct of Method Transfer Studies for Type C Medicated Feed Assay Methods | Guideline Explorer | BioRegHub