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Content and Format of Composition Statement and Corresponding Statement of Ingredients in Labeling in NDAs and ANDAs

DraftCenter for Drug Evaluation and Research04/29/2024
Bioequivalence

Description

The Food and Drug Administration (FDA or Agency) is announcing the availability of a draft guidance for industry entitled “Content and Format of Composition Statements in NDAs and ANDAs and Corresponding Statement of Ingredients in Labeling.”  This guidance is intended to assist new drug application (NDA) and abbreviated new drug application (ANDA) applicants in submitting an accurate and complete composition statement in their applications and corresponding statement of ingredients in the labeling, when applicable.  This guidance describes best practices for writing the composition statement and corresponding statement of ingredients in labeling.  This guidance recommends how applicants can provide complete information with the goal of minimizing the number of assessment cycles and communications that are necessary for approval, as well as ensuring product labels are written clearly.

Key Topics

Terms and concepts identified from this document

Scope & Applicability

Product Classes

1
Reference Listed Drug

The drug product identified by the applicant for comparison; Comparison of ANDA product to RLD for pH adjuster differences

Stakeholders

1
Applicant

Entity submitting development data and knowledge; Entity performing the work process for change

Regulatory Context

Regulatory Activities

2
NDA

New Drug Application

ANDA

Abbreviated New Drug Application

Document Types

10
Composition Statement

Information submitted in a drug product's NDA or ANDA

DESCRIPTION Section

Specific section of the Prescribing Information for ingredient listing

Annual Report

Reporting category for minor changes like removing a color additive

Statement of Ingredients

Information contained in a drug product's DESCRIPTION section of its prescribing information

Prescribing Information

The primary section of drug labeling where SLCs are implemented

Master Batch Records

Records used to ensure consistency in composition

Annual Reports

Reports containing drug product compositions

eCTD Section 3.2.P.1

Location of the drug product composition statement

Master Production Records

Records in section 3.2.R that must be consistent with composition statements

Drug Master File

A submission to FDA that may be used to provide confidential information about facilities or processes.; cross-referencing a DMF in a BLA

Attributes

7
Qualitative (Q1)

Ingredient information regarding identity

tonicity adjuster

Information not required by regulation but recommended for inclusion

pH adjuster

Functionality of sodium hydroxide in labeling

Quantitative (Q2)

Ingredient information regarding amount

Q1 sameness

Qualitative sameness of inactive ingredients

Q2 sameness

Quantitative sameness of inactive ingredients

Hydration state

Property of inactive ingredients that must be identified in the application; Applicants should list the ingredients' hydration state(s)

Technical Details

Substances

10
Inactive Ingredient

Referenced by non-combination product regulatory submissions in more than one center.

sodium hydroxide

Added for in situ conversion and pH adjustment

hydrochloric acid

Added to adjust pH

water for injection

Inactive ingredient/vehicle listed in the example

sodium metabisulfate

Inactive ingredient listed in the example

sodium citrate

Inactive ingredient listed in the example

sodium chloride

Inactive ingredient listed in the example

povidone K-17

Inactive ingredient listed in the example

citric acid monohydrate

Inactive ingredient listed in the example

sodium drugozide

Salt form equivalent of the active ingredient

Processes

2
Manufacture

The process for which all components must be listed

in situ conversion

composition table should indicate the amount used for in situ conversion

Standards & References

External Standards

4
USP General Chapter <1091>

See USP General Chapter <1091> Labeling of Inactive Ingredients.

United States Pharmacopeia

Official compendium for device recognition

USP General Notices 3.20

USP General Notices 3.20, Indicating Conformance.

USP-NF

Standard for inactive ingredient titles and monographs; Anhydrous and dihydrate terms are consistent with USP-NF monograph terminology.

Specifications

1
not less than 99.5 percent and not more than 100.5 percent

USP purity standard for citric acid

Related CFR Sections (9)

Enforcement Impact

Deficiencies cited in Warning Letters referencing the same regulations

misbranded drugs
1
failure to disclose undeclared ingredients
1
misbranded drugs under section 502
1
unapproved new drugs sold in violation of sections 505(a) and 301(d)
1
Introduction of unapproved new drugs into interstate commerce
1
Introduction of misbranded drugs into interstate commerce
1
Unapproved new drugs
1
Misbranded drugs
1
Unapproved new drug
1
unapproved new drugs introduced into interstate commerce
1

Related Warning Letters (5)

See Also (8)

Content and Format of Composition Statement and Corresponding Statement of Ingredients in Labeling in NDAs and ANDAs | Guideline Explorer | BioRegHub