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Q4B Annex 8: Sterility Test General Chapter

FinalCenter for Biologics Evaluation and Research Center for Drug Evaluation and Research12/22/2009

Description

This annex is one in a series of guidance documents that describe the evaluations and recommendations by the Q4B Expert Working Group (EWG) of selected pharmacopoeial texts to facilitate their recognition by regulatory authorities for use as interchangeable in the ICH regions. Implementation of the Q4B annexes is intended to avoid redundant testing by industry. For general information on the Q4B process, the reader is referred to the core guidance Q4B Evaluation and Recommendation of Pharmacopoeial Texts for Use in the ICH Regions.

Key Topics

Terms and concepts identified from this document

Scope & Applicability

Product Classes

2
Liquid parenteral preparations

Specific container sampling requirements for batches

Medical devices

Subject to mandatory recall provisions

Stakeholders

3
Manufacturers

Responsible for declaring acceptable market names on labels.

Sponsors

Assist sponsors in the nonclinical evaluation

Q4B Expert Working Group

Evaluates selected pharmacopoeial texts for recognition

Regulatory Context

Regulatory Activities

3
Marketing Authorization Application

Submissions supported by clinical trial data.

Prior approval procedures

Regulatory mechanisms for method changes

Change notification

Handling compendial changes

Document Types

1
PDG Stage 5B sign-off document

The PDG Stage 5B sign-off document: Japanese Pharmacopoeial Forum

Technical Details

Substances

1
Diluting and rinsing fluids

Should not have antibacterial or antifungal properties

Testing Methods

1
Sterility Test

Test performed at release

Standards & References

External Standards

6
JP 4.06

Japanese Pharmacopoeia Sterility Test

USP <71>

Sterility testing may be performed in accordance with USP <71>.

Ph. Eur. Chapter 2.6.1

European Pharmacopoeia Sterility monograph

USP <71> Sterility Tests

United States Pharmacopeia sterility test text

JP 4.06 Sterility Test

Japanese Pharmacopoeia sterility test text

Ph. Eur. 2.6.1. Sterility

European Pharmacopoeia sterility test text

Specifications

1
Acceptance Criteria

limits for solid state form and particle size; Tightening acceptance criteria; Numerical limits or ranges for tests

ICH References (2)

ICH Q4B Annex 8

Sterility Test General Chapter evaluation for interchangeability

ICH Q4B

Evaluation and Recommendation of Pharmacopoeial Texts

See Also (8)

Q4B Annex 8: Sterility Test General Chapter | Guideline Explorer | BioRegHub